Hydrogen permeation measurement of the reduced activation ferritic steel F82H by the vacuum thermo-balance method

Yoshida, Hajime; Kosaku, Yasuo*; Enoeda, Mikio; Abe, Tetsuya; Akiba, Masato

JAERI-Research 2005-003, 13 Pages, 2005/03

JAERI-Research-2005-003.pdf:3.33MB

Hydrogen permeation fluxes of the reduced activation ferritic steel F82H were quantitatively measured by a newly proposed method, vacuum thermo-balance method, for a precise estimation of tritium leakage in a fusion reactor. We prepared sample capsules made of F82H, which enclosed hydrogen gas. The hydrogen in the capsules permeated through the capsule wall, and subsequently desorbed from the capsule surface during isothermal heating. The vacuum thermo-balance method allows simultaneous measurement of the hydrogen permeation flux by two independent methods, namely, the net weight reduction of the sample capsule and exhaust gas analysis. Thus the simultaneous measurements by two independent methods increase the reliability of the permeability measurement. The ratio of the hydrogen permeation fluxes obtained by the net weight reduction to that measured by the exhaust gas analysis was in the range from 1/4 to 1/1 in this experiment. It has been demonstrated that the vacuum thermo-balance method is effective for the measurement of hydrogen permeation rate of F82H.